安捷伦Infiniti II高效液相色谱和SCIEX6500+系统
| 日期: | 03/24/2017 |
| 类别: |
仅用于科研，不用于诊断
回答
关于安捷伦HPLC与6500+联机问题，可以参考下面步骤重新建立联接以及创建新方法。
1.去活hardware profile，关闭Analyst®软件，重启Analyst软件。
2.打开Analyst软件，点开Analyst装置驱动（ADD），检查液相色谱仪状态。如果没有连接成功，需要关闭ADD及重启液相色谱仪。
3.确定ADD中的液相图标都不是灰色，则可以关闭ADD状态栏及窗口。
4. 激活hardware profile，ADD软件会自动打开。
5. 建议打开ADD的状态栏确定一下连接。
6. 关闭ADD状态栏，但不能关闭ADD窗口。
7.在Analyst新建一个方法，并确保Sync中选择了Manual/AAO。
8. 填入质谱参数。
9. 在Analyst保存并关闭方法。
10.到ADD窗口中的Method模块。
11. 开打刚刚新建的Analyst方法，文件名后缀为.dam。
12.输入合适的液相条件，确保输入STOP TIME。建议STOP TIME放在泵参数的同一页中。
13. 保存Analyst方法文件，后缀为 .dam。
14. 在ADD上关闭方法模块。
15. 使用Analyst打开该方法， LC参数应该有相应的显示。
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